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This test method covers the use of both pyridine and pyridine-free KF reagents for determining water by the volumetric titration. Determination of water using KF coulometric . application of the volumetric Karl Fischer (KF) titration for determining free water and water of hydration in most solid or liquid organic and inorganic compounds.This standard has been approved for use by agencies of the U.S. Department of Defense. 1. Scope . 2.1 ASTM Standards:2 . D4177 Practice for Automatic Sampling of Petroleum and Petroleum Products E203 Test Method for Water Using Volumetric Karl Fischer Titration 2.2 API Standards:3 MPMS Chapter 8.1 Manual Sampling of Petroleum and Petroleum . 7 Karl Fischer Reagent is available from various laboratory suppliers. Pyridine-free adaptations are available and may be used if precision can be established. If you are aware of alternative suppliers, please provide this information to ASTM International Headquarters. Your comments will receive careful consideration at a
This standard has been approved for use by agencies of the Department of Defense. 1. Scope* 1.1 This test method is intended as a general guide for the application of the volumetric Karl Fischer (KF) titration for determining free water and water of hydration in most solid or . 2.1 A list of existing ASTM Karl Fischer methods, their .
This standard has been approved for use by agencies of the U.S. Department of Defense. . 1.1 This test method is intended as a general guide for the application of the volumetric Karl Fischer (KF) titration for determining free water and water of hydration in most solid or . 2.1 A list of existing ASTM Karl Fischer methods, their . 4.1 The coulometric technique is especially suited for determining low concentrations of water in organic liquids that would yield small titers by the Karl Fischer volumetric procedure. The precision and accuracy of the coulometric technique decreases for concentrations of water much greater than 2.0 % because of the difficulty in measuring the .1.1 This test method is intended as a general guide for the application of the volumetric Karl Fischer (KF) titration for determining free water and water of hydration in most solid or liquid organic and inorganic compounds. This test method is designed for use with automatic titration systems capable of determining the KF titration end point potentiometrically; however, a .specimen injected into the titration cell shall be calibrated. NOTE 1—The use of balances on structures that are in motion may not be appropriate. 7.5 Titration Cell—Sunlight can cause disassociation of the iodine in the Karl Fischer reagent, resulting in false results. A titration cell made of opaque material may reduce this effect. 8.
ASTM E203-01 Standard Test Method for Water Using Volumetric Karl Fischer Titration. 1.1 This test method is intended as a general guide for the application of the volumetric Karl Fischer (KF) titration for determining free water and water of hydration in most solid or liquid organic and inorganic compounds. This test method is designed for use .lometric Karl Fischer Titration E180 Practice for Determining the Precision of ASTM Methods for Analysis and Testing of Industrial and Spe-cialty Chemicals (Withdrawn 2009)3 E1064 Test Method for Water in Organic Liquids by Coulo-metric Karl Fischer Titration 3. Summary of Test Method 3.1 The sample, containing a maximum of 100 mg of water, Standard Test Method for Water in Lint Cotton by Oven Evaporation Combined with Volumetric Karl Fischer Titration D7785-12 ASTM|D7785-12 . ASTM grants Licensee a limited, revocable, nonexclusive, non-transferable license to access, by means of one or more authorized IP addresses, and according to the terms of this Agreement, to make the uses . Scope1.1 This test method is intended as a general guide for the application of the volumetric Karl Fischer (KF) titration for determining free water and water of hydration in most solid or liquid organic and inorganic compounds. This test method is desig . ASTM grants Licensee a limited, revocable, nonexclusive, non-transferable license to .
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Standard Test Method for Water Using Volumetric Karl Fischer Titration 1. Gennaro Sannino. . This standard has been approved for use by agencies of the Department of Defense. . Referenced Documents 2.1 A list of existing ASTM Karl Fischer methods, their applications to various products, and the sponsoring committees is given in Appendix X3 . Scope1.1 This test method is intended as a general guide for the application of the volumetric Karl Fischer (KF) titration for determining free water and water of hydration in most solid or liquid organic and inorganic compounds. This test method is desig . ASTM grants Licensee a limited, revocable, nonexclusive, non-transferable license to . Standard Test Method for Water in Crude Oils by Coulometric Karl Fischer Titration D4928-12R18 ASTM|D4928-12R18 . Internet traffic volume, upgrades, overload of requests to servers, general network failures or delays, or any other cause that may from time to time make the Product unavailable for the Licensee or Licensee's Authorized Users. .
Titration techniques using KF reagent are one of the most widely used for the determination of water. Although the volumetric KF titration can determine low levels of water, it is generally accepted that coulometric KF titrations (see Test Method E 1064) are more accurate for routine determination of very low levels of water.As a general rule, if samples routinely . based on ASTM E203, Standard Test Method for Water Using Volumetric Karl Fischer Titration [3]. This standard test method is specified for measuring the mass % water in pyrolysis liquid biofuels in ASTM D7544, Standard Specification for Pyrolysis Liquid Biofuel [4]. Although the standard method is prescribed for the analysis of pyrolysisASTM E203: Volumetric Karl Fischer Titration ASTM E203 test provides a general guide to determine free water and water of hydration in most solid or liquid organic a nd inorganic compounds using volumetric Karl Fischer (KF) .
Water in Solids by Furnace Desorption with Volumetric Karl Fischer Titration UOP993-15 UOP . ASTM grants Licensee a limited, revocable, nonexclusive, non-transferable license to access, by means of one or more authorized IP addresses, and according to the terms of this Agreement, to make the uses permitted and described below, each ASTM .
USA Testing Lab for ASTM E203 Water Content Analysis Using Volumetric Karl Fischer Titration in USA, Indonesia, Philippines, Malaysia, Thailand, Canada, China, India, and all over the World. (302)244-7710 . [email protected] . FREE Consultation Services . Materials testing . contact ASTM Customer Service at [email protected]. For Annual Book of ASTM Standards volume information, refer to the standardÕs Document Summary page on the ASTM website. 3 Scholz, E., ÒKarl-Fischer Titration,Ó Springer-Verlag, Berlin, Heidelberg, New York, Tokyo, 1984, 140 pp. 4.1 The coulometric technique is especially suited for determining low concentrations of water in organic liquids that would yield small titers by the Karl Fischer volumetric procedure. The precision and accuracy of the coulometric technique decreases for concentrations of water much greater than 2.0 % because of the difficulty in measuring the .The optimum pH range of the sample solution for efficient Karl Fischer titration is between pH 5.5 and 8. When the pH is greater than 8.5, the reaction rate increases due to chemical side reactions. . This is then titrated using the ASTM D6304 procedure. Because additives and other interfering contaminants that may be present in a used oil .
This standard has been approved for use by agencies of the Department of Defense. 1. Scope . 2.1 ASTM Standards: 2 . D4177 Practice for Automatic Sampling of Petroleum and Petroleum Products E203 Test Method for Water Using Volumetric Karl Fischer Titration 2.2 API Standards: 3 MPMS Chapter 8.1 Manual Sampling of Petroleum and Petroleum .Titration; Karl Fischer titration; coulo KFC; water metric; content determination; ASTM E 1064 . Summary This Application Bulletin gives an overview of the coulometric water content determination according to Karl Fischer. . The same chemical processesas in a volumetric KF titration take place , i.e.1 mol H,2O consumes 1mol of I . 2. As theASTM E203-08 Standard Test Method for Water Using Volumetric Karl Fischer Titration. 1.1 This test method is intended as a general guide for the application of the volumetric Karl Fischer (KF) titration for determining free water and water of hydration in most solid or liquid organic and inorganic compounds. This test method is designed for use .
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This standard has been approved for use by agencies of the U.S. Department of Defense. . 1.1 This test method is intended as a general guide for the application of the volumetric Karl Fischer (KF) titration for determining free water and water of hydration in most solid or . 2.1 A list of existing ASTM Karl Fischer methods, their . Standard Practice for Water in Lint Cotton by Oven Evaporation Combined with Volumetric Karl Fischer Titration D7785-21 ASTM|D7785-21 . ASTM grants Licensee a limited, revocable, nonexclusive, non-transferable license to access, by means of one or more authorized IP addresses, and according to the terms of this Agreement, to make the uses .
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astm volumetric karl fischer titration agencies|karl fischer titration mettler toledo